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Clarity - Getting Started First “Analysis”
32
The calibration file (*.CAL) used for identifiing
and quantitating the peaks is linked by its
name in the template method and
consequently in the chromatogram method.
In the next step we will prepare template
method for new chromatograms with general
acquisition parameters.
Later, after measuring the chromatogram, we
will modify further parameters (e.g. integration
table) in the chromatogram method.
Finally we will save the changed chromatogram
method as a template method.
5.3.1 Measurement and evaluation parameters
Comments
Certain parameters (voltage range, sampling
rate etc.) must be set prior to measurement
.
Caution! Changing of these parameters is blocked during
measurement because it would render the
measurement void.
Proceed
Create a new NONAME method using the File -
New Method in the
Instrument.
Place the cursor over the chromatograph icon
to change the image to four icons.
Clicking on one of the circled icons will display
the contents of the current template method in
the
Method Setup dialog (see Chapter 4.3 -
Method Setup dialog on pg. 21).
On the
Measurement tab, fill in the description of
the chromatographic conditions and set up the
Enable Autostop, Run Time and External
Start/Stop options.
On the
Acquisition tab, set up the Range and
Sample Rate according to your detector
output and expected peak widths.
Note: The peaks exceeding the specified range will be
cut and the respective area lost, however lower
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